HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethylpyridine → 4-Ethylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethylpyridine | HCID 10822 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Ethylpyridine | HCID 10822 | — |
| Product | 4,4'-Diethyl-2,2'-bipyridine | HCID 21822330 | — |
Reaction Steps
1 gram (g) of 5% or 10% palladium-on-carbon catalyst and 25 milliliters (ml) 4-ethylpyridine are heated for 3 days under reflux while being stirred. (Alternatively, 5% platinum-on-carbon or 5% rhodium-on-carbon may be used as the catalyst.) The reaction mixture is treated with boiling benzene, filtered, and distilled to give benzene, 4-ethylpyridine, and 4,4'-diethyl-2,2'-bipyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05846702 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-3cbd3f970b3341d1a876eefb17420eeb |
| Source note | uspto-grants-1998_12 |