HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonylamine → 6,7-dichloro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonylamine | HCID 2723901 | — |
| Reactant | 6,7-dichloro-1H-indole | HCID 12272802 | — |
| Product | 6,7-dichloro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole | HCID 18545981 | 89.8% |
Reaction Steps
Beginning with 1.4 gm (7.5 mMol) 6,7-dichloro-1H-indole and 2.3 gm (15.0 mMol) 4-piperidone hydrochloride monohydrate, 1.8 gm (89%) of the title compound were recovered as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05846982 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-ea03b541e2524d34811130f13dc83771 |
| Source note | uspto-grants-1998_12 |