HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methyl-2-piperidone → 5-bromo-3-(1-methyl-1,2,3,6-tetrahydro-4-pyridinyl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methyl-2-piperidone | HCID 13603 | — |
| Reactant | 5-Bromoindole | HCID 24905 | — |
| Product | 5-bromo-3-(1-methyl-1,2,3,6-tetrahydro-4-pyridinyl)-1H-indole | HCID 14973208 | 100.1% |
Reaction Steps
Following the procedure described in detail in Example 1, 30.0 gm (0.153 mole) 5-bromoindole and 38 mL (0.306 mole) 1-methylpiperidone were reacted together to prepare 44.6 gm (100%) of the desired compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05846982 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-fce189a0828548f5bb0be1ba7ed27967 |
| Source note | uspto-grants-1998_12 |