Ethylamine → HCID 21221556, compound

HRID 1457076Notes

Reaction equation

HRID 1457076 reaction equation
[CH3:1][N:2]([CH3:19])[CH:3]1[CH2:18][CH2:17][C:6]2[O:7][C:8]3[CH:13]=[CH:12][C:11]([C:14](Cl)=[O:15])=[CH:10][C:9]=3[C:5]=2[CH2:4]1.[CH2:20]([NH2:22])[CH3:21]>>[CH2:20]([NH:22][C:14]([C:11]1[CH:12]=[CH:13][C:8]2[O:7][C:6]3[CH2:17][CH2:18][CH:3]([N:2]([CH3:19])[CH3:1])[CH2:4][C:5]=3[C:9]=2[CH:10]=1)=[O:15])[CH3:21]

Participants

3

Reactant 2

HCID 6341EthylamineHCID 21221671HCID 21221671, compound

Product 1

HCID 21221556HCID 21221556, compoundYield 33%

Procedure

Beginning with 0.011 gm (0.04 mMol) 2-dimethylamino-1,2,3,4-tetrahydrodibenzofuran-8-carbonyl chloride and 0.08 mMol ethylamine, 0.0037 gm (33%) of the title compound were recovered.

Sources & evidence

ORD record
ord-c22a28cbaaf04b4787a9c9ff0ac8bab4
Source dataset
uspto-grants-1998_12
Patent number
US05846995

Reaction notes

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