HCID 131720968, compound → HCID 19361972, compound

HRID 1457165Notes

Reaction equation

HRID 1457165 reaction equation
[C:1]([C:4]1[CH:28]=[CH:27][C:7]([O:8][CH2:9][CH:10]([OH:26])[CH2:11][S:12][C:13]2[CH:18]=[CH:17][C:16]([CH2:19][C:20]([O:22]C)=[O:21])=[C:15]([Cl:24])[C:14]=2[Cl:25])=[C:6]([CH2:29][CH2:30][CH3:31])[C:5]=1[OH:32])(=[O:3])[CH3:2].C(C1C=CC(OCCCSC2C=CC(CC(OC)=O)=C(Cl)C=2Cl)=C(CCC)C=1O)(=O)C>>[C:1]([C:4]1[CH:28]=[CH:27][C:7]([O:8][CH2:9][CH:10]([OH:26])[CH2:11][S:12][C:13]2[CH:18]=[CH:17][C:16]([CH2:19][C:20]([OH:22])=[O:21])=[C:15]([Cl:24])[C:14]=2[Cl:25])=[C:6]([CH2:29][CH2:30][CH3:31])[C:5]=1[OH:32])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 131720968HCID 131720968, compoundHCID 131720969HCID 131720969, compound

Product 1

HCID 19361972HCID 19361972, compound

Procedure

By following Step H of Example 1, but substituting the product of Step A of this example for the ester of Step G of Example 1, the title compound, mp 151°-153° C., was obtained.

Sources & evidence

ORD record
ord-877e3d358fb3406c881a0cccb15caca1
Source dataset
uspto-grants-1998_12
Patent number
US05847008

Reaction notes

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