HCID 131720969, compound → HCID 19361985, compound

HRID 1457166Notes

Reaction equation

HRID 1457166 reaction equation
[C:1]([C:4]1[CH:29]=[CH:28][C:7]([O:8][CH2:9][CH2:10][CH2:11][S:12]([C:15]2[CH:20]=[CH:19][C:18]([CH2:21][C:22]([O:24]C)=[O:23])=[C:17]([Cl:26])[C:16]=2[Cl:27])(=[O:14])=[O:13])=[C:6]([CH2:30][CH2:31][CH3:32])[C:5]=1[OH:33])(=[O:3])[CH3:2].C(C1C=CC(OCCCSC2C=CC(CC(OC)=O)=C(Cl)C=2Cl)=C(CCC)C=1O)(=O)C>>[C:1]([C:4]1[CH:29]=[CH:28][C:7]([O:8][CH2:9][CH2:10][CH2:11][S:12]([C:15]2[CH:20]=[CH:19][C:18]([CH2:21][C:22]([OH:24])=[O:23])=[C:17]([Cl:26])[C:16]=2[Cl:27])(=[O:14])=[O:13])=[C:6]([CH2:30][CH2:31][CH3:32])[C:5]=1[OH:33])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 131720969HCID 131720969, compoundHCID 131720970HCID 131720970, compound

Product 1

HCID 19361985HCID 19361985, compound

Procedure

By following Step H of Example 1, but substituting the product of Step A of this example for the ester of Step G of Example 1, the title compound, mp 180°-181° C., was obtained.

Sources & evidence

ORD record
ord-4d7513aab4f941ce94cf30a777e7b8a7
Source dataset
uspto-grants-1998_12
Patent number
US05847008

Reaction notes

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