HCID 131720969, compound → HCID 19361990, compound

HRID 1457167Notes

Reaction equation

HRID 1457167 reaction equation
[C:1]([C:4]1[CH:30]=[CH:29][C:7]([O:8][CH2:9][CH:10]([OH:28])[CH2:11][S:12]([C:15]2[CH:20]=[CH:19][C:18]([CH2:21][C:22]([O:24]C)=[O:23])=[C:17]([Cl:26])[C:16]=2[Cl:27])(=[O:14])=[O:13])=[C:6]([CH2:31][CH2:32][CH3:33])[C:5]=1[OH:34])(=[O:3])[CH3:2].C(C1C=CC(OCCCSC2C=CC(CC(OC)=O)=C(Cl)C=2Cl)=C(CCC)C=1O)(=O)C>>[C:1]([C:4]1[CH:30]=[CH:29][C:7]([O:8][CH2:9][CH:10]([OH:28])[CH2:11][S:12]([C:15]2[CH:20]=[CH:19][C:18]([CH2:21][C:22]([OH:24])=[O:23])=[C:17]([Cl:26])[C:16]=2[Cl:27])(=[O:14])=[O:13])=[C:6]([CH2:31][CH2:32][CH3:33])[C:5]=1[OH:34])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 131720969HCID 131720969, compoundHCID 131720971HCID 131720971, compound

Product 1

HCID 19361990HCID 19361990, compound

Procedure

By following Step H of Example 1, but substituting the product from Step A of this example for the ester of Step G of Example 1, the title compound, mp 181°-183° C., was obtained.

Sources & evidence

ORD record
ord-7a066f03b7214bb49a52731bac56997e
Source dataset
uspto-grants-1998_12
Patent number
US05847008

Reaction notes

Loading…