HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-((tert-Butoxycarbonyl)amino)hexanoic acid → HCID 22104045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-((tert-Butoxycarbonyl)amino)hexanoic acid | HCID 637602 | — |
| Reactant | Glycine ethyl ester, hydrochloride | HCID 2723640 | — |
| Product | HCID 22104045 | HCID 22104045 | 127.8% |
Reaction Steps
By working analogously to what described in example 2, 6-(tert-butoxycarbonylamino)hexanoic acid (163 g) was directly condensed with glycine ethyl ester hydrochloride (118 g; 0.845 moles), obtaining thus N-[6-(tert-butoxycarbonylamino)hexanoyl]glycine ethyl ester (285 g) as a raw product which was used as such in the subsequent reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05847092 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-1d5e4b4246624771aae786b6d5279a2a |
| Source note | uspto-grants-1998_12 |