4-Methoxybenzoic Acid → HCID 22104009, compound

HRID 1457229Notes

Reaction equation

HRID 1457229 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=O)=[CH:5][CH:4]=1.[CH2:12]([O:14][C:15](=[O:26])[CH2:16][NH:17][C:18](=[O:25])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][NH2:24])[CH3:13]>>[CH2:12]([O:14][C:15](=[O:26])[CH2:16][NH:17][C:18](=[O:25])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][NH:24][C:7](=[O:9])[C:6]1[CH:5]=[CH:4][C:3]([O:2][CH3:1])=[CH:11][CH:10]=1)[CH3:13]

Participants

3

Reactant 2

HCID 74784-Methoxybenzoic AcidHCID 22104012HCID 22104012, compound

Product 1

HCID 22104009HCID 22104009, compound

Procedure

By working analogously to what described in example 2 and by using 4-methoxybenzoic acid (33 mmoles) and N-(6-aminohexanoyl)glycine ethyl ester (39.5 mmoles), prepared as described in example 3, N-[6-[(4-methoxybenzoyl)amino]hexanoyl]glycine ethyl ester was obtained as a crude product, used as such in the subsequent reactions.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-83de966b64304cbcb797c19c9637853f
Source dataset
uspto-grants-1998_12
Patent number
US05847092

Reaction notes

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