HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 4-(4-Methoxyphenyl)phenethyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-{4-(4-Methoxyphenyl) phenyl}ethylbenzylether | HCID 53955301 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-(4-Methoxyphenyl)phenethyl alcohol | HCID 2759704 | 92% |
Reaction Steps
2,59 g (7.85 mol) of 2-{4-(4-methoxyphenyl) phenyl}ethylbenzylether, 0.4 g of 5% palladium activated carbon, 70 ml of ethanol and 6 ml of dioxane were injected and stirred at room temperature for 7 hours under presence of hydrogen. After the reactions had been completed, the catalyst was removed by tuck filtration and the solvent was removed by filtration so that 1.64 g of 2-{4-(4-methoxyphenyl) phenyl}ethanol was obtained (yield 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849217 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-c15176df31134fd98a711e5d8363c520 |
| Source note | uspto-grants-1998_12 |