HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22099567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 15288194 | HCID 15288194 | — |
| Reactant | 6-(5-Fluoro-2-methylbenzoyl)aminopyridine-3-carbonyl chloride | HCID 15508250 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22099567 | HCID 22099567 | — |
Reaction Steps
As described for Example 1, 9,10-dihydro-4-H-thieno[2,3-c][1]benzazepine in dichloromethane, in the presence of triethylamine is reacted with 6-[(5-fluoro-2-methylbenzoyl)amino]pyridine-3-carbonyl chloride to give the product as a non-crystalline yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849735 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-edbbf0fd3efd4ffc873ac377d0fd9f11 |
| Source note | uspto-grants-1998_12 |