6-[([1,1'-Biphenyl]-2-ylcarbonyl)amino]-3-pyridinecarbonyl chloride → HCID 22099843, compound
Reaction equation
[CH3:1][N:2]1[CH:15]=[C:5]2[CH2:6][CH2:7][NH:8][C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[C:4]2=[N:3]1.[C:16]1([C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[C:22]([NH:24][C:25]1[N:30]=[CH:29][C:28]([C:31](Cl)=[O:32])=[CH:27][CH:26]=1)=[O:23]>>[CH3:1][N:2]1[CH:15]=[C:5]2[CH2:6][CH2:7][N:8]([C:31]([C:28]3[CH:27]=[CH:26][C:25]([NH:24][C:22]([C:17]4[C:16]([C:34]5[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=5)=[CH:21][CH:20]=[CH:19][CH:18]=4)=[O:23])=[N:30][CH:29]=3)=[O:32])[C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[C:4]2=[N:3]1Participants
3
Procedure
As described for Example 12, 2,4,5,6-tetrahydro-2-methylpyrazolo[4,3-d][1]benzazepine is reacted with 6-[([1,1'biphenyl]-2-ylcarbonyl)amino]-3-pyridinecarbonyl chloride to give the product as a solid.
Sources & evidence
- ORD record
- ord-73dacb070aa843faa87eeeaf3fb3548f
- Source dataset
- uspto-grants-1998_12
- Patent number
- US05849735
Reaction notes
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