10,11-Dihydro-5h-dibenzo[b,e][1,4]diazepine → HCID 22099553, compound

HRID 1457680Notes

Reaction equation

HRID 1457680 reaction equation
[CH:1]1[C:11]2[CH2:10][NH:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[NH:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH3:16][C:17]1[O:18][CH:19]=[CH:20][C:21]=1[C:22]([NH:24][C:25]1[N:30]=[CH:29][C:28]([C:31](Cl)=[O:32])=[CH:27][CH:26]=1)=[O:23]>>[CH:1]1[C:11]2[CH2:10][N:9]([C:31]([C:28]3[CH:27]=[CH:26][C:25]([NH:24][C:22]([C:21]4[CH:20]=[CH:19][O:18][C:17]=4[CH3:16])=[O:23])=[N:30][CH:29]=3)=[O:32])[C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[NH:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 3604610,11-Dihydro-5h-dibenzo[b,e][1,4]diazepineHCID 22099840HCID 22099840, compound

Product 1

HCID 22099553HCID 22099553, compound

Procedure

As described for Example 20, 5,11-dihydro-10H-dibenz[b,e][1,4]diazepine is reacted with 6-[(2-methyl-3-furanylcarbonyl)amino]-3-pyridinecarbonyl chloride to give the product as a solid.

Sources & evidence

ORD record
ord-a3dda82c3c774786a0bab1a001422cc6
Source dataset
uspto-grants-1998_12
Patent number
US05849735

Reaction notes

Loading…