4-Phenylbenzoyl chloride → HCID 22099560, compound

HRID 1457684Notes

Reaction equation

HRID 1457684 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][CH2:7][NH:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:16]1([C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)[CH:21]=[CH:20][C:19]([C:22](Cl)=[O:23])=[CH:18][CH:17]=1>>[C:16]1([C:25]2[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=2)[CH:17]=[CH:18][C:19]([C:22]([N:6]2[CH2:7][CH2:8][C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[C:11]3[CH:1]=[CH:2][CH:3]=[CH:4][C:5]2=3)=[O:23])=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 841514-Phenylbenzoyl chlorideHCID 13497478HCID 13497478, compound

Product 1

HCID 22099560HCID 22099560, compound

Procedure

As described for Example 26, 6,7-dihydro-5H-dibenz[b,d]azepine is reacted with [1,1'-biphenyl]-4-carbonyl chloride to give the product as a solid.

Sources & evidence

ORD record
ord-33d52a1868e3494a85e381a8aa34b1b6
Source dataset
uspto-grants-1998_12
Patent number
US05849735

Reaction notes

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