10,11-Dihydrodibenzo(b,f)(1,4)oxazepine → HCID 22099860, compound

HRID 1457686Notes

Reaction equation

HRID 1457686 reaction equation
[CH:1]1[C:6]2[CH2:7][NH:8][C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[O:11][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:16]([C:24]1[CH:32]=[CH:31][C:27]([C:28](Cl)=[O:29])=[CH:26][CH:25]=1)(=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:16]([C:24]1[CH:25]=[CH:26][C:27]([C:28]([N:8]2[CH2:7][C:6]3[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=3[O:11][C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]2=3)=[O:29])=[CH:31][CH:32]=1)(=[O:23])[C:17]1[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=1

Participants

3

Reactant 2

HCID 64893310,11-Dihydrodibenzo(b,f)(1,4)oxazepineHCID 129121414-Benzoylbenzoyl chloride

Product 1

HCID 22099860HCID 22099860, compound

Procedure

As described for Example 26, 10,11-dihydrodibenz[b,f][1,4]oxazepine is reacted with 4-(benzoyl)benzoyl chloride to give the product as an off-white, m.p. 103°-106° C.; Mass spectrum (CI), 406 (MH+).

Workup

  1. customto give the product as an off-white, m.p. 103°-106° C.

Sources & evidence

ORD record
ord-a76fe6af64e044bbaa8def447f61c73f
Source dataset
uspto-grants-1998_12
Patent number
US05849735

Reaction notes

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