4,10-Dihydro-5H-thieno[3,2-c][1]benzazepine → HCID 22099764, compound

HRID 1457689Notes

Reaction equation

HRID 1457689 reaction equation
[S:1]1[C:10]2[CH2:9][C:8]3[CH:11]=[CH:12][CH:13]=[CH:14][C:7]=3[NH:6][CH2:5][C:4]=2[CH:3]=[CH:2]1.[C:15]([C:23]1[CH:31]=[CH:30][C:26]([C:27](Cl)=[O:28])=[CH:25][CH:24]=1)(=[O:22])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[C:15]([C:23]1[CH:24]=[CH:25][C:26]([C:27]([N:6]2[C:7]3[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=3[CH2:9][C:10]3[S:1][CH:2]=[CH:3][C:4]=3[CH2:5]2)=[O:28])=[CH:30][CH:31]=1)(=[O:22])[C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 108673664,10-Dihydro-5H-thieno[3,2-c][1]benzazepineHCID 129121414-Benzoylbenzoyl chloride

Product 1

HCID 22099764HCID 22099764, compound

Procedure

As described for Example 26, 4,10dihydro-5H-thieno[3,2-c][1]benzazepine is reacted with 4-(benzoyl)benzoyl chloride to give the product as a solid.

Sources & evidence

ORD record
ord-424e9950640243a18e75c4f75f9fee6f
Source dataset
uspto-grants-1998_12
Patent number
US05849735

Reaction notes

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