HCID 22099770, compound → HCID 22099625, compound
Reaction equation
[CH:1]1[S:2][CH:3]=[C:4]2[C:10]=1[CH2:9][NH:8][C:7]1[CH:11]=[CH:12][CH:13]=[CH:14][C:6]=1[NH:5]2.[C:15]1([C:33]2[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=2)[C:16]([C:21]([NH:23][C:24]2[N:29]=[CH:28][C:27](C(Cl)=O)=[CH:26][CH:25]=2)=[O:22])=[CH:17][CH:18]=[CH:19][CH:20]=1>>[CH:1]1[S:2][CH:3]=[C:4]2[C:10]=1[CH2:9][N:8]([C:27]1[CH:26]=[CH:25][C:24]([NH:23][C:21]([C:16]3[C:15]([C:33]4[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=4)=[CH:20][CH:19]=[CH:18][CH:17]=3)=[O:22])=[N:29][CH:28]=1)[C:7]1[CH:11]=[CH:12][CH:13]=[CH:14][C:6]=1[NH:5]2Participants
3
Procedure
As described for Example 400, 9,10-dihydro-4H-thieno[3,4-b][1,5]benzodiazepine is reacted with 6-[([1,1'-biphenyl]-2-carbonyl)amino]-pyridine-3-carbonyl chloride to give the product as a solid.
Sources & evidence
- ORD record
- ord-3a6bc46f8c5c4396a88fdba4c876aac2
- Source dataset
- uspto-grants-1998_12
- Patent number
- US05849735
Reaction notes
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