HCID 22100400, compound → HCID 70204293, compound

HRID 1457787Notes

Reaction equation

HRID 1457787 reaction equation
Br[N:2]1[C:6]2=[N:7][C:8]([CH3:11])=[CH:9][CH:10]=[C:5]2[NH:4][CH:3]1[CH2:12][CH2:13][CH2:14][CH3:15].[CH:16](OB(O)O)=[CH:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[CH2:12]([C:3]1[NH:4][C:5]2[C:6]([N:2]=1)=[N:7][C:8]([CH3:11])=[C:9]([CH:16]=[CH:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[CH:10]=2)[CH2:13][CH2:14][CH3:15]

Participants

3

Reactant 2

HCID 22100400HCID 22100400, compoundHCID 54113416HCID 54113416, compound

Product 1

HCID 70204293HCID 70204293, compoundYield 103.2%

Procedure

The same procedure as in step 8 of Example 1 was repeated using 4.0 g(0.0133 mole) of the compound obtained in step 4 of Example 1 and 3.0 g(0.0203 mole) of styrylboric acid to obtain 4.0 g of the title compound(yield 93%).

Sources & evidence

ORD record
ord-d25735af1b124cc8b90b00d5adce035e
Source dataset
uspto-grants-1998_12
Patent number
US05849753

Reaction notes

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