HCID 11107379, compound → HCID 53857075, compound

HRID 1457829Notes

Reaction equation

HRID 1457829 reaction equation
[C:1]([O:4][CH2:5][C@@H:6]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[CH3:18])[CH2:7][O:8]C(=O)C)(=[O:3])[NH2:2].C(OC[C@@H](C1C=CC=CC=1)COC(=O)C)(=O)N>>[C:1]([O:4][CH2:5][C@@H:6]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[CH3:18])[CH2:7][OH:8])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 11107379HCID 11107379, compoundHCID 67572608HCID 67572608, compound

Product 1

HCID 53857075HCID 53857075, compoundYield 78.3%

Procedure

The title compound was synthesized in a similar manner to that of Example XXII, except that (S)-3-acetoxy-2-(o-methylphenyl)propanol carbamate, instead of (S)-3-acetoxy-2-phenylpropanol carbamate, was used as a starting material. Yield 78.3%. Purity 99.0%.

Sources & evidence

ORD record
ord-4a0cbc73795b49c98f296c18f894db1c
Source dataset
uspto-grants-1998_12
Patent number
US05849772

Reaction notes

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