HCID 11107379, compound → HCID 54135201, compound

HRID 1457831Notes

Reaction equation

HRID 1457831 reaction equation
[C:1]([O:4][CH2:5][C@@H:6]([C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][C:13]=1[O:20][CH3:21])[CH2:7][O:8]C(=O)C)(=[O:3])[NH2:2].C(OC[C@@H](C1C=CC=CC=1)COC(=O)C)(=O)N>>[C:1]([O:4][CH2:5][C@@H:6]([C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][C:13]=1[O:20][CH3:21])[CH2:7][OH:8])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 11107379HCID 11107379, compoundHCID 67572920HCID 67572920, compound

Product 1

HCID 54135201HCID 54135201, compoundYield 65.3%

Procedure

The title compound was synthesized in a similar manner to that of Example XXII, except that (S)-3-acetoxy-2-(2,4-dimethoxyphenyl)propanol carbamate, instead of (S)-3-acetoxy-2-phenylpropanol carbamate, was used as a starting material. Yield 65.3%. Purity 99.2%.

Sources & evidence

ORD record
ord-7195daf1741d4fbc984bf71b3b90ca55
Source dataset
uspto-grants-1998_12
Patent number
US05849772

Reaction notes

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