HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethylhydrazine → HCID 57178595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethylhydrazine | HCID 5976 | — |
| Reactant | HCID 18630184 | HCID 18630184 | — |
| Product | HCID 57178595 | HCID 57178595 | 81% |
Reaction Steps
The acid prepared in Example 203 was converted to the acid chloride by the procedure of example b. The acid chloride was reacted with 1,1-dimethylhydrazine using General Method E1 to afford the title compound. Purification by recrystallization from ether/hexanes gave 0.62 g of the title compound as off-white crystals in 81% yield. m.p. 144°-145° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849723 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-8823a23a879346df840683b1ef002f31 |
| Source note | uspto-grants-1998_12 |