反应详情

2.68 g of Z-Pal-N(Me)Bzl (6.85 mMol) are dissolved in 30 ml of MeOH and after adding 0.3 g of Pd-carbon hydrogenated for 5 hours at ambient temperature and 5 bar. Then, the mixture is filtered, the filtrate is concentrated on the rotary evaporator, the residue is dissolved in ether, filtered and the filtrate is again concentrated. H-Pal-N(Me)Bzl is obtained as a light green oil.

1. filtrationThen, the mixture is filtered
2. concentrationthe filtrate is concentrated on the rotary evaporator
3. dissolutionthe residue is dissolved in ether
4. filtrationfiltered
5. concentrationthe filtrate is again concentrated