HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 14457497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,6-Octadiene, 1-bromo-3,7-dimethyl-, (2E)- | HCID 5365867 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14457497 | HCID 14457497 | — |
Reaction Steps
To a solution of methyl 4- hydroxybenzoate (33.2 g) in acetone (300 ml) were added geranyl bromide (44.5 g) and potassium carbonate (55.2 g). The mixture was refluxed with heating for 2 hours. The reaction solution, after water (200 ml) were added thereto, was extracted with chloroform (400 ml). The extract was dried over sodium sulfate anhydride and then concentrated under a vacuum to yield a raw product of methyl 4-geranyloxybenzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849930 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-30650a178a5a418bb4a8bb53edba7850 |
| Source note | uspto-grants-1998_12 |