HRID1458318

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3283

Diethyl Ether

C4H10O

2 次

$结构：CC(=O)OC/C(=C(\C(=O)O)c1ccccc1)c1ccc(S(C)(=O)=O)cc1$

HCID11617716

未命名化合物

PRODUCTS

生成物

$结构：COC(=O)/C(=C(\COC(C)=O)c1ccc(S(C)(=O)=O)cc1)c1ccccc1$

HCID23211915

未命名化合物

PROCEDURE

实验过程

To a suspension of the acid from Example 4 (100 mg) in Et2O (20 mL) was added dropwise excess CH2N2 solution in Et2O. The solution was concentrated and the solid was swished with 2:1 hexane/EtOAc to give 90 mg of the title compound as a white solid.

WORKUP

后处理

concentrationThe solution was concentrated