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HRID1458671

反应详情

EQUATION

反应方程式

HRID 1458671 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)S(F)(F)F
HCID123472

Diethylaminosulfur trifluoride

C4H10F3NS

结构：CCc1ncnc(N[C@H]2CC[C@@H](C(C)(C)C)CC2)c1C(=O)OC
HCID178437726

未命名化合物

结构：CCc1ncnc(N[C@H]2CC[C@@H]([Si](C)(C)C)CC2)c1CO
HCID178437737

未命名化合物

PRODUCTS

生成物

1
结构：CCc1ncnc(N[C@H]2CC[C@@H](C(C)(C)C)CC2)c1CF
HCID178437719

未命名化合物

PROCEDURE

实验过程

This compound can be prepared starting from 5-carbomethoxy-4-(cis-4-tert-butylcyclohexylamino)-6-ethylpyrimidine (Example 5) by reduction to the 5-hydroxymethyl compound (in analogy to Example 37) and fluorination with diethylaminosulfur trifluoride (DAST).

WORKUP

后处理

  1. customThis compound can be prepared