Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 2-Chloro-1-fluoro-4-nitrobenzene | HCID 67688 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 10491618 | HCID 10491618 | 63.9% |
Reaction Steps
Dissolved in 8 ml of DMSO were 10.0 g (57.0 mmol) of 3-chloro-4-fluronitrobenzene and 8.6 g (82 mmol) of diethanolamine. The thus-obtained mixture was stirred under heat for 2 hours at 140° C., followed by extraction with ethyl acetate. The solvent was distilled out under reduced pressure, whereby 9.5 g of the title compound were obtained as a yellow oil (yield: 64%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05852011 |
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| Source dataset | uspto-grants-1998_12 |
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| ORD ID | ord-e150a9436f40469f87ce6544e1a81a8e |
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| Source note | uspto-grants-1998_12 |
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