Diethanolamine → HCID 15683610, compound

Participants

Reaction Conditions

Reaction Steps

Dissolved in 4 ml of DMSO were 1.0 g (3.69 mmol) of N-(2-nitro-5-chlorobenzoyl)morpholine and 1.16 g (11 mmol) of diethanolamine. The resulting mixture was stirred under heat at 140° C. for 3 hours. After the reaction, the reaction mixture was concentrated and the resulting yellow syrup was purified by chromatography on a silica gel column (chloroform/methanol=10/1), whereby 667 mg of the title compound were obtained as yellow powder (yield: 53.5%).

Provenance & Evidence