HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22097227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 22097215 | HCID 22097215 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | HCID 22097227 | HCID 22097227 | — |
Reaction Steps
A solution 1.4 g (4.8 mmol) of N-(2-chloro-4,5-diacetamidophenyl)pyrrole and 0.4 g (9.8 mmol) of potassium hydroxide in 25 ml of ethylene glycol was stirred at 60° C. for 30 minutes. The reaction mixture was then poured into water, extracted with ethyl acetate and worked up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05852017 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-b5aeb035bbc04359a7ae943f1de7c367 |
| Source note | uspto-grants-1998_12 |