2,5-Dimethoxytetrahydrofuran → 6-(1-Pyrrolyl)-7-nitro-2,3(1H,4H)-quinoxalinedione

HRID 1458805Notes

Reaction equation

HRID 1458805 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][C:11]=1[N+:12]([O-:14])=[O:13])[NH:8][C:7](=[O:15])[C:6](=[O:16])[NH:5]2.CO[CH:19]1[CH2:23][CH2:22][CH:21](OC)O1>>[N:1]1([C:2]2[CH:3]=[C:4]3[C:9](=[CH:10][C:11]=2[N+:12]([O-:14])=[O:13])[NH:8][C:7](=[O:15])[C:6](=[O:16])[NH:5]3)[CH:19]=[CH:23][CH:22]=[CH:21]1

Participants

3

Reactant 2

HCID 790982,5-DimethoxytetrahydrofuranHCID 39809926-Amino-7-nitroquinoxaline-2,3-diol

Product 1

HCID 220971056-(1-Pyrrolyl)-7-nitro-2,3(1H,4H)-quinoxalinedione

Procedure

23.2 mmol of 6-amino-7-nitro-2,3(1H,4H)-quinoxalinedione were reacted with 23.2 mmol of 2,5-dimethoxytetrahydrofuran by the method of Example 5d.

Sources & evidence

ORD record
ord-a0ed4d6886d348608ee4e66e6c227c89
Source dataset
uspto-grants-1998_12
Patent number
US05852017

Reaction notes

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