HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → HCID 22097139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | HCID 22097170 | HCID 22097170 | — |
| Product | HCID 22097139 | HCID 22097139 | 76% |
Reaction Steps
35 g (0.124 mol) of 2-amino-4-chloro-N-(2-ethylbutyl)aniline were refluxed in 350 ml of diethyl oxalate for 2.5 h. After cooling, the precipitate was filtered off with suction and dried to yield 33 g (76%) of the product. Melting point 253°-255°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05852017 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-263714afd02141a2898675e9af27087d |
| Source note | uspto-grants-1998_12 |