HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl borate → [4-(Nonyloxy)phenyl]boronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl borate | HCID 8470 | — |
| Reactant | 4-n-Octyloxyphenylboronic Acid (contains varying amounts of Anhydride) | HCID 3977284 | — |
| Reactant | HCID 14640447 | HCID 14640447 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | [4-(Nonyloxy)phenyl]boronic acid | HCID 4197997 | — |
Reaction Steps
Quantities: compound 27 (14.70 g, 0.066 mol) in anhydrous THF (140 ml), n-butyllithium (30 ml, 2.5M in hexane, 0.075 mol), trimethyl borate (13.72 g, 0.132 mol) in anhydrous THF (50 ml). The experimental procedure was as described for the preparation of compound 33.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05853613 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-fabcc536a60946ac996a141221922789 |
| Source note | uspto-grants-1998_12 |