Benzene, (3-iodopropyl)- → HCID 22723606, compound

HRID 1459101Notes

Reaction equation

HRID 1459101 reaction equation
[I:1][CH2:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[CH2:11]([C:23]1[CH:28]=[CH:27][N:26]=[CH:25][CH:24]=1)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>CC(C)=O>[I-:1].[C:5]1([CH2:4][CH2:3][CH2:2][N+:26]2[CH:27]=[CH:28][C:23]([CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[CH:24][CH:25]=2)[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

4

Reactant 2

HCID 138121Benzene, (3-iodopropyl)-HCID 13811458HCID 13811458, compound

Product 1

HCID 22723606HCID 22723606, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

The compound was synthesized by boiling a mixture of 2.26 g (9.2 mmol) 1-iodo-3-phenyl propane and 2,57 g (10.0 mmol) 4-n-dodecylpyridine in 35 ml of dry acetone for 16 hours. The solvent was evaporated and the yellow solid substance was recrystallized from THF/ether. The yield is 3.06 g (6.2 mmol), melting point 79.0°-80.0° C.

Workup

  1. customThe compound was synthesized
  2. customThe solvent was evaporated
  3. customthe yellow solid substance was recrystallized from THF/ether

Sources & evidence

ORD record
ord-d0601e9a8b324226bd845f17a38b2cbc
Source dataset
uspto-grants-1998_12
Patent number
US05853694

Reaction notes

Loading…