Ammonium Chloride → HCID 178479028, compound

HRID 1459181Notes

Reaction equation

HRID 1459181 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH:6]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH2:7][CH2:8][N:9]=1.[Cl-:16].[NH4+:17]>CO>[ClH:16].[C:10]1([CH:6]2[CH2:7][CH2:8][NH:9][C:3](=[NH:17])[CH2:4][CH2:5]2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 15453852HCID 15453852, compound

Product 1

HCID 178479028HCID 178479028, compoundYield 94.6%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 30 (17 g, 8.6 mmol) in 20 mL of MeOH was reacted with ammonium chloride (0.43 g, 8.0 mmol) by the method of EXAMPLE 27 to yield 1.7 g (91%) of the title material.

Sources & evidence

ORD record
ord-4a4a38c48f89463784bbb12d30d965fa
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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