Ammonium Chloride → HCID 178430627, compound

HRID 1459182Notes

Reaction equation

HRID 1459182 reaction equation
CO[C:3]1[CH2:4][CH:5]([CH3:11])[CH2:6][CH:7]([CH3:10])[CH2:8][N:9]=1.[Cl-:12].[NH4+:13]>CO>[ClH:12].[CH3:11][CH:5]1[CH2:6][CH:7]([CH3:10])[CH2:8][NH:9][C:3](=[NH:13])[CH2:4]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 15453854HCID 15453854, compound

Product 1

HCID 178430627HCID 178430627, compoundYield 92.1%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 34 (1.75 g, 8.6 mmol) in 25 mL of MeOH was reacted with ammonium chloride (0.48 g, 9.0 mmol) by the method of EXAMPLE 27 to yield 1.4 g (83%) of the title material.

Sources & evidence

ORD record
ord-358eb438072d4c42b58214afadb2e8c6
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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