Ammonium Chloride → HCID 178425009, compound

HRID 1459183Notes

Reaction equation

HRID 1459183 reaction equation
CO[C:3]1[CH:4]([CH3:11])[CH2:5][CH2:6][CH2:7][CH:8]([CH3:10])[N:9]=1.[Cl-:12].[NH4+:13]>CO>[ClH:12].[CH3:11][CH:4]1[CH2:5][CH2:6][CH2:7][CH:8]([CH3:10])[NH:9][C:3]1=[NH:13]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 15453857HCID 15453857, compound

Product 1

HCID 178425009HCID 178425009, compoundYield 102.4%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 38 (1.24 g, 8.0 mmol) in 25 mL of MeOH was reacted with ammonium chloride (0.37 g, 6.8 mmol) by the method of EXAMPLE 27 to yield 1.23 g (91%) of the title material.

Sources & evidence

ORD record
ord-45f798a53a37470eb2f46bc09ed6aa14
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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