Ammonium Chloride → HCID 178425480, compound

HRID 1459185Notes

Reaction equation

HRID 1459185 reaction equation
CO[C:3]1[CH:4]([CH3:10])[CH2:5][CH2:6][CH2:7][CH2:8][N:9]=1.[Cl-:11].[NH4+:12]>CO>[ClH:11].[CH3:10][CH:4]1[CH2:5][CH2:6][CH2:7][CH2:8][NH:9][C:3]1=[NH:12]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 12348081HCID 12348081, compound

Product 1

HCID 178425480HCID 178425480, compoundYield 79.9%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 44 (294 mg, 2.1 mmol) in 14.5 mL of MeOH was reacted with ammonium chloride (103 mg, 2.0 mmol) by the method of EXAMPLE 27 to yield 260 mg (77%) of the title material.

Sources & evidence

ORD record
ord-e0b4233fe72242a3b45dd130af5c2a2f
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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