Ammonium Chloride → HCID 178436358, compound

HRID 1459189Notes

Reaction equation

HRID 1459189 reaction equation
[CH2:1]([CH:3]1[C:9](OC)=[N:8][CH2:7][CH2:6][CH2:5][CH2:4]1)[CH3:2].[Cl-:12].[NH4+:13]>CO>[ClH:12].[CH2:1]([CH:3]1[CH2:4][CH2:5][CH2:6][CH2:7][NH:8][C:9]1=[NH:13])[CH3:2]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 10606998HCID 10606998, compound

Product 1

HCID 178436358HCID 178436358, compoundYield 93.5%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 58 (600 mg, 3.9 mmol) in 20 mL of MeOH was reacted with ammonium chloride (165 mg, 3.1 mmol) by the method of EXAMPLE 27 to yield 512 mg (93%) of the title material.

Sources & evidence

ORD record
ord-1a71a8abd707469988c7905eba35c993
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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