Ammonium Chloride → HCID 178425252, compound

HRID 1459190Notes

Reaction equation

HRID 1459190 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH2:6][C:7]([CH3:11])([CH3:10])[CH2:8][N:9]=1.[Cl-:12].[NH4+:13]>CO>[ClH:12].[CH3:10][C:7]1([CH3:11])[CH2:8][NH:9][C:3](=[NH:13])[CH2:4][CH2:5][CH2:6]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428605HCID 18428605, compound

Product 1

HCID 178425252HCID 178425252, compoundYield 91.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 63 (490 mg, 3.2 mmol) in 18 mL of MeOH was reacted with ammonium chloride (125 mg, 2.4 mmol) by the method of EXAMPLE 27 to yield 387 mg (69%) of the title material.

Sources & evidence

ORD record
ord-e676eb37321446899304695f62a4796e
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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