Ammonium Chloride → HCID 178428578, compound

HRID 1459192Notes

Reaction equation

HRID 1459192 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH:6]([CH3:10])[CH2:7][CH2:8][N:9]=1.[Cl-:11].[NH4+:12]>CCO>[ClH:11].[CH3:10][CH:6]1[CH2:7][CH2:8][NH:9][C:3](=[NH:12])[CH2:4][CH2:5]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 1060683639985-26-7

Product 1

HCID 178428578HCID 178428578, compoundYield 81.2%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product of EXAMPLE 69 (750 mg, 5.3 mmol) in 3 mL of EtOH was reacted with ammonium chloride (285 mg, 5.3 mmol) by the method of EXAMPLE 27 to yield 700 mg (77%) of the title material.

Sources & evidence

ORD record
ord-147452703ad14fd5ad109731ab0250d9
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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