Ammonium Chloride → HCID 178441158, compound

HRID 1459195Notes

Reaction equation

HRID 1459195 reaction equation
[CH3:1][C:2]([CH:5]1[CH2:11][CH2:10][C:9](OC)=[N:8][CH2:7][CH2:6]1)([CH3:4])[CH3:3].[Cl-:14].[NH4+:15]>CCO>[ClH:14].[CH3:1][C:2]([CH:5]1[CH2:6][CH2:7][NH:8][C:9](=[NH:15])[CH2:10][CH2:11]1)([CH3:4])[CH3:3]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 12604432HCID 12604432, compound

Product 1

HCID 178441158HCID 178441158, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product of EXAMPLE 83 (2.5 g, 13.6 mmol) in 50 mL of EtOH was reacted with ammonium chloride (730 mg, 13.6 mmol) by the method of EXAMPLE 27 to yield 2.2 g (78%, of the title material.

Workup

  1. customto yield 2.2 g (78%

Sources & evidence

ORD record
ord-0be22ce99d304c82bf0d44e0e6011748
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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