Ammonium Chloride → HCID 178440909, compound

HRID 1459198Notes

Reaction equation

HRID 1459198 reaction equation
[CH3:1][C:2]([CH:5]1[C:11](OC)=[N:10][CH2:9][CH2:8][CH2:7][CH2:6]1)([CH3:4])[CH3:3].[Cl-:14].[NH4+:15]>CO>[ClH:14].[CH3:1][C:2]([CH:5]1[CH2:6][CH2:7][CH2:8][CH2:9][NH:10][C:11]1=[NH:15])([CH3:4])[CH3:3]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428484HCID 18428484, compound

Product 1

HCID 178440909HCID 178440909, compoundYield 63.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 99 (551 mg, 2.7 mmol) in 10 mL of MeOH was reacted with ammonium chloride (145 mg, 2.7 mmol) by the method of EXAMPLE 27 to yield 350 mg of the crude title material.

Sources & evidence

ORD record
ord-532c74619f4b434ebb33fe9af12377dc
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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