Ammonium Chloride → HCID 178439140, compound

HRID 1459200Notes

Reaction equation

HRID 1459200 reaction equation
CO[C:3]1[CH:4]([CH2:10][CH:11]=[CH2:12])[CH2:5][CH2:6][CH2:7][CH2:8][N:9]=1.[Cl-:13].[NH4+:14]>CO>[ClH:13].[CH2:10]([CH:4]1[CH2:5][CH2:6][CH2:7][CH2:8][NH:9][C:3]1=[NH:14])[CH:11]=[CH2:12]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 10607182HCID 10607182, compound

Product 1

HCID 178439140HCID 178439140, compoundYield 78.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 105 (90 mg, 0.54 mmol) in 10 mL of MeOH was reacted with ammonium chloride (24.5 mg, 0.46 mmol) by the method of EXAMPLE 27 to yield 68 mg (67%) of the title material.

Sources & evidence

ORD record
ord-ae125bd45302474ba74f6f9b4fc659ea
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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