Ammonium Chloride → HCID 178439141, compound

HRID 1459202Notes

Reaction equation

HRID 1459202 reaction equation
CO[C:3]1[CH:4]([CH2:10][CH2:11][CH3:12])[CH2:5][CH2:6][CH2:7][CH2:8][N:9]=1.[Cl-:13].[NH4+:14]>CO>[ClH:13].[CH2:10]([CH:4]1[CH2:5][CH2:6][CH2:7][CH2:8][NH:9][C:3]1=[NH:14])[CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 12348082HCID 12348082, compound

Product 1

HCID 178439141HCID 178439141, compoundYield 89.9%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 111 (415 mg, 2.45 mmol) in 20 mL of MeOH was reacted with ammonium chloride (111 mg, 2.1 mmol) by the method of EXAMPLE 27 to yield 360 mg (76%) of the title material.

Sources & evidence

ORD record
ord-857ee7702cb84c7a843e250a6b806ffc
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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