Ammonium Chloride → HCID 178439095, compound

HRID 1459203Notes

Reaction equation

HRID 1459203 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH2:10][CH2:11][CH3:12])[N:9]=1.[Cl-:13].[NH4+:14]>CO>[ClH:13].[CH2:10]([CH:8]1[NH:9][C:3](=[NH:14])[CH2:4][CH2:5][CH2:6][CH2:7]1)[CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 10583266HCID 10583266, compound

Product 1

HCID 178439095HCID 178439095, compoundYield 96.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 112 (560 mg, 3.3 mmol) in 20 mL of MeOH was reacted with ammonium chloride (150 mg, 2.8 mmol) by the method of EXAMPLE 27 to yield 514 mg (78%) of the title material.

Sources & evidence

ORD record
ord-3b67446417354a628d016dd65319f1ab
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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