Ammonium Chloride → HCID 178428577, compound

HRID 1459206Notes

Reaction equation

HRID 1459206 reaction equation
CO[C:3]1[CH2:4][CH:5]([CH3:11])[CH:6]([CH3:10])[CH2:7][CH2:8][N:9]=1.[Cl-:12].[NH4+:13]>CO>[ClH:12].[CH3:11][CH:5]1[CH:6]([CH3:10])[CH2:7][CH2:8][NH:9][C:3](=[NH:13])[CH2:4]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428537HCID 18428537, compound

Product 1

HCID 178428577HCID 178428577, compoundYield 66%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 123 (100 mg, 0.64 mmol) in 5 mL of MeOH was reacted with ammonium chloride (29.3 mg, 547 mmol) by the method of EXAMPLE 27 to yield 68 mg (66%) of the white solid title material.

Sources & evidence

ORD record
ord-ffa7c601f43a4fa7b8f78bd36bfc11cc
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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