Ammonium Chloride → HCID 178425544, compound

HRID 1459209Notes

Reaction equation

HRID 1459209 reaction equation
CO[C:3]1[CH2:4][CH:5]([CH3:11])[CH2:6][CH2:7][CH:8]([CH3:10])[N:9]=1.[Cl-:12].[NH4+:13]>CCO>[ClH:12].[CH3:11][CH:5]1[CH2:6][CH2:7][CH:8]([CH3:10])[NH:9][C:3](=[NH:13])[CH2:4]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428471HCID 18428471, compound

Product 1

HCID 178425544HCID 178425544, compoundYield 77.8%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product of EXAMPLE 130 (250 mg, 1.6 mmol) in 2.5 mL of EtOH was reacted with ammonium chloride (86.0 mg, 1.6 mmol) by the method of EXAMPLE 27 to yield 220 mg (75%) of the white solid title material.

Sources & evidence

ORD record
ord-d9791694e8fb4cee92a26bf0328f2d4d
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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