Ammonium Chloride → HCID 178479038, compound

HRID 1459227Notes

Reaction equation

HRID 1459227 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[N:9]=1.[Cl-:16].[NH4+:17]>CO>[ClH:16].[C:10]1([CH:8]2[NH:9][C:3](=[NH:17])[CH2:4][CH2:5][CH2:6][CH2:7]2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 10822028HCID 10822028, compound

Product 1

HCID 178479038HCID 178479038, compoundYield 90.5%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 191 (1.4 g, 6.9 mmol) in 75 mL of MeOH was reacted with ammonium chloride (0.31 g, 5.9 mmol) by the method of EXAMPLE 27 to yield 1.2 g (77%) of the title material.

Sources & evidence

ORD record
ord-f644f461bd60435db4cddc12a352b897
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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