Ammonium Chloride → HCID 178440872, compound

HRID 1459277Notes

Reaction equation

HRID 1459277 reaction equation
CO[C:3]1[CH2:9][CH2:8][CH2:7][CH2:6][CH:5]([CH:10]=[CH:11][CH2:12][CH3:13])[N:4]=1.[Cl-:14].[NH4+:15]>CO>[ClH:14].[CH:10]([CH:5]1[NH:4][C:3](=[NH:15])[CH2:9][CH2:8][CH2:7][CH2:6]1)=[CH:11][CH2:12][CH3:13]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 54379138HCID 54379138, compound

Product 1

HCID 178440872HCID 178440872, compoundYield 101.6%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of Example 327 (1.5 g, 8 mmol) in 85 mL of MeOH was reacted with ammonium chloride (0.36 g, 6.8 mmol) by the method of Example 27 to yield 1.4 g (83%) of the title material.

Sources & evidence

ORD record
ord-3ebd591ab8734d52aef0d5edc34c330d
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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