HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[(E)-2,4-pentadienyl]-N-(2-propenyl)-acetamide → 8-Azabicyclo[4.3.0]non-2-ene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[(E)-2,4-pentadienyl]-N-(2-propenyl)-acetamide | HCID 12260271 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 8-Azabicyclo[4.3.0]non-2-ene | HCID 12386767 | — |
Reaction Steps
Dissolve 33.1 g (0.2 mol) of N-[(E)-2,4-pentadienyl]-N-(2-propenyl)-acetamide (title compound of Example A.3.) in 200 ml of xylene, pass through a vigorous stream of nitrogen for 15 min, add 0.1 g of 4-hydroxyanisole, then reflux overnight. Concentrate and distil under a high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05854241 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-00e2b42907cc411c89a21e81e10dc24e |
| Source note | uspto-grants-1998_12 |