HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N-[4-(6,7-Dihydro-dibenzo[b,d]azepine-5-carbonyl)-phenyl]-2-methyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-[(2-methylbenzoyl)amino]benzoyl Chloride | HCID 10707441 | — |
| Reactant | 5H-Dibenz[b,d]azepine | HCID 16070162 | — |
| Product | N-[4-(6,7-Dihydro-dibenzo[b,d]azepine-5-carbonyl)-phenyl]-2-methyl-benzamide | HCID 44212554 | — |
Reaction Steps
As described for EXAMPLE 2, 1 mmol of 4-[(2-methylbenzoyl)amino]benzoyl chloride, 1 mmol of 5H-dibenz[b,d]azepine and 2 mmol of triethylamine are stirred at room temperature for 5 hours to give the product as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05854236 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-5bf20f0dba63424eb31235e9490cdbb7 |
| Source note | uspto-grants-1998_12 |